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毛建友教授课题组在Organic Letters发表研究论文
 添加时间:2021/05/19 发布:

Palladium-Catalyzed Direct Arylation of 2-Pyridylmethyl Silanes with Aryl Bromides

Tingzhi Lin,1 Pengcheng Qian, 1 Yan-En Wang, 2 Mingjie Ou, 1 Long Jiang, 3 Chen Zhu, 1 Yuchuan Xu, 1 Dan Xiong,1 and Jianyou Mao,*, 1

1Technical Institute of Fluorochemistry (TIF), Institute of Advanced Synthesis, School of Chemistry and Molecular Engi-neering, Nanjing Tech University, 30 South Puzhu Road, Nanjing 211800, P. R. China.

2College of Science, Hebei Agricultural University, Baoding 071000, P. R. China.

3Institute of Advanced Synthesis (IAS), Northwestern Polytechnical University (NPU), Xi'an, 710072, China. Yangtze River Delta Research Institute of NPU, Taicang Jiangsu, 215400, P. R. China.

Abstract: The first palladium-catalyzed direct arylation of 2-pyridylmethyl silanes with aryl bromides to generate a diverse array of aryl(pyridyl)-methyl silane derivatives has been developed. This protocol facilitates access to various kinds of heterocycle-containing silanes in good to excellent yields (40 examples, 6697% yield) with good functional group tolerance. The scalability of this transformation is demonstrated.

 

DOI:10.1021/acs.orglett.1c00677 (2020年影响因子: 6.091).

论文链接:https://pubs.acs.org/doi/10.1021/acs.orglett.1c00677

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